- CAS
- Purity
- 18600-42-5
- 99%
Quality products?make an important contribution to long-term revenue and profitability. Offer Chemical Raw Material 4-Nitrobenzylamine hydrochloride 18600-42-5 In Stock
4-Nitrobenzylamine hydrochloride was used in chemical modification of graphite powder and multiwalled carbon nanotubes. It was also used in the preparation of 2-fluoro-6-(4-nitrohenzylamino)purine.
4-nitrobenzonitrile
4-nitrobenzylamine hydrochloride
| Conditions | Yield |
|---|---|
|
4-nitrobenzonitrile;
With
C46H178O41Si42; titanium(IV)isopropoxide;
In
toluene;
at 60 ℃;
for 9h;
Inert atmosphere;
With
hydrogenchloride; water;
In
toluene;
at 20 ℃;
Reagent/catalyst;
chemoselective reaction;
Inert atmosphere;
|
90%
|
|
4-nitrobenzonitrile;
With
titanium(IV) isopropylate; 1,1,3,3-Tetramethyldisiloxane;
In
toluene;
at 60 ℃;
for 24h;
Inert atmosphere;
With
hydrogenchloride;
In
water;
at 20 ℃;
|
86%
|
|
With
hydrogenchloride; diborane;
Multistep reaction;
2) ether;
|
|
|
Multi-step reaction
with
2
steps
1: tris(pentafluorophenyl)borate / chloroform-d1 / 0.17 h / 85 °C / Inert atmosphere
2: hydrogenchloride; water / diethyl ether / 1 h / 20 °C
With
hydrogenchloride; tris(pentafluorophenyl)borate; water;
In
diethyl ether; chloroform-d1;
|
4-nitrobenzamide
4-nitrobenzylamine hydrochloride
| Conditions | Yield |
|---|---|
|
4-nitrobenzamide;
With
[(aNHC)KN(SiMe3)2]2; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane;
In
toluene;
at 40 ℃;
for 12h;
Inert atmosphere;
Glovebox;
Schlenk technique;
With
water; sodium hydroxide;
In
diethyl ether; toluene;
at 40 ℃;
for 1h;
Inert atmosphere;
Glovebox;
Schlenk technique;
With
hydrogenchloride;
In
diethyl ether; water;
Reagent/catalyst;
chemoselective reaction;
Inert atmosphere;
Glovebox;
Schlenk technique;
|
83%
|
|
4-nitrobenzamide;
With
bis(tetrahydrofuran)calcium di(bis(trimethylsilyl)amide); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane;
In
toluene;
at 120 ℃;
for 36h;
Inert atmosphere;
Schlenk technique;
With
hydrogenchloride;
In
diethyl ether; toluene;
Inert atmosphere;
Schlenk technique;
|
71%
|
|
Yield given. Multistep reaction;
|
|
|
Multi-step reaction
with
2
steps
1: lithium 2,6-di-tert-butylphenolate / neat (no solvent) / 18 h / 60 °C / Inert atmosphere; Glovebox; Schlenk technique
2: sodium hydroxide / water; diethyl ether / 1 h
With
lithium 2,6-di-tert-butylphenolate; sodium hydroxide;
In
diethyl ether; water;
|
|
|
Multi-step reaction
with
2
steps
1: La(CH2
C6
H4
NMe2
-o)3
on SBA-15 / toluene / 24 h / 120 °C / Schlenk technique; Inert atmosphere
2: hydrogenchloride / ethyl acetate; diethyl ether / 20 °C / Schlenk technique; Inert atmosphere
With
hydrogenchloride;
In
diethyl ether; ethyl acetate; toluene;
|
The CAS number of 4-Nitrobenzylamine hydrochloride is 18600-42-5.
More information of 4-Nitrobenzylamine hydrochloride 18600-42-5 are:
|
CAS?Number |
18600-42-5 |
|
Melting Point |
~265 °C (dec.)(lit.) |
|
Boiling Point |
297.5°C at 760 mmHg |
|
Flash Point |
133.7°C |
|
Vapor Pressure |
0.00135mmHg at 25°C |
|
HS CODE |
29214990 |
|
PSA |
71.84000 |
|
LogP |
3.07900 |
Synonyms?for?4-Nitrobenzylamine hydrochloride 18600-42-5:Benzenemethanamine,4-nitro-, monohydrochloride (9CI);Benzylamine, p-nitro-, hydrochloride(6CI,7CI);Benzylamine, p-nitro-, monohydrochloride (8CI);p-Nitrobenzylamine hydrochloride;
The chemical formula of ?4-Nitrobenzylamine hydrochloride is?C7H8N2O2. HCl which containing 7 Carbon atoms,9 Hydrogen atoms,2 Nitrogen atoms,1 Oxygen atoms and 1 Chlorine atoms,and the molecular weight of??4-Nitrobenzylamine hydrochloride?is 188.614.
4-Nitrobenzylamine hydrochloride is a light brown crystalline solid that is commonly utilized in various chemical reactions and modifications due to its unique properties.
InChI:InChI=1/C7H8N2O2/c8-5-6-1-3-7(4-2-6)9(10)11/h1-4H,5,8H2/p+1
Relevant articles related to 4-Nitrobenzylamine hydrochloride:
|
Article |
Source |
|
Lithium compound catalyzed deoxygenative hydroboration of primary, secondary and tertiary amides |
Bisai, Milan Kumar,Gour, Kritika,Das, Tamal,Vanka, Kumar,Sen, Sakya S. , p. 2354 - 2358 (2021/03/03) |
|
Fabrication of ω-Transaminase@Metal-Organic Framework Biocomposites for Efficiently Synthesizing Benzylamines and Pyridylmethylamines |
Chen, Lina,Ding, Yingying,Jiao, Qingcai,Liu, Junzhong,Yu, Jinhai,Zhang, Hongjuan,Zong, Weilu , (2021/11/05) |
Hebei Xixun Trading Co.,Ltd is a quality supplier of 4-Nitrobenzylamine hydrochloride. Our main goal is customer satisfaction. Contact us to negotiate the best price for your business on 4-Nitrobenzylamine hydrochloride 18600-42-5.